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SiC/Nb/SiC扩散连接接头的界面构造及接合强度
冯吉才, 刘会杰, 韩胜阳, 李卓然, 张九海
哈尔滨工业大学
摘要:
使用Nb箔作中间层对常压烧结SiC陶瓷进行了真空扩散连接。在最初的反应阶段,六方晶的Nb2C和Nb5Si3Cx反应物分别在Nb和Si侧形成。随着连接时间的增加,立方晶的NbC和六方晶的NbSi2相在界面出现。试验结果表明,在1790K、36ks的连接条件下所获得的接头,其室温剪切强度达到187MPa,高温(973K)剪切强度超过150MPa。
关键词:  扩散连接  界面反应  接合强度  碳化硅陶瓷
DOI:
分类号:
基金项目:国家博士后基金
Interface Structures and Bonding Strength of SiC/Nb/SiC Diffusion Bonded Joint
Feng Jicai, Liu Huijie, Han Shengyang, Li Zhuoran, Zhang Jiuhai
Harbin Institute of Technology
Abstract:
Pressureless-sintered (PLS) SiC was bonded to SiC through Nb foil interlayer by vaccum diffusion method.At the initial stage of reaction,a hexagonal Nb2C phase and a hexagonal Nb5Si3Cx phase occured on the Nb side and on the SiC side,respectively.With the increase in bonding time,a cubic NbC phase and a hexagonal NbSi2 phase appeared at the interface.The experimental results showed that shear strengrh of the joint,which was bonded at 1790 K for 36ks,was up to 187 MPa at room temperature and more than 150 MPa at the test tempeature of 973 K.
Key words:  diffusion bonding  interface reaction  bonding strength  SiC ceramic